dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

Base Information

Chemical Name:dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)
CAS No.:189263-49-8
Molecular Formula:C₂₃H₁₉N₅O₄
Molecular Weight:429.435
Hs Code.:

Synonyms:dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

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Chemical Property of dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

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Technology Process of dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

There total 4 articles about dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 100-44-7
benzyl chloride

: 189263-48-7
dimethyl 6,6'-(1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

: 189263-49-8
dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

Guidance literature:: With potassium carbonate; In acetonitrile; for 4h; Heating;
DOI:10.1002/hlca.19970800204

Reference yield:

: 150223-77-1
2,2'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pirydine)

: 189263-49-8
dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / CH₂Cl₂ / 48 h

2: AcOH, H₂SO₄ / 2 h / Heating

3: 1) SOCl₂ / 1) 15 min,, RT, 2) reflux, 5 h

4: 76 percent / K₂CO₃ / acetonitrile / 4 h / Heating

With thionyl chloride; sulfuric acid; potassium carbonate; acetic acid; In dichloromethane; acetonitrile;
DOI:10.1002/hlca.19970800204

Reference yield:

: 150223-78-2
1-benzyl-3,5-bis(6'-cyano-2'-pyridyl)-1,2,4-triazole

: 189263-49-8
dimethyl 6,6'-(1-benzyl-1H-1,2,4-triazole-3,5-diyl)bis(pyridine-2-carboxylate)

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH, H₂SO₄ / 2 h / Heating

2: 1) SOCl₂ / 1) 15 min,, RT, 2) reflux, 5 h

3: 76 percent / K₂CO₃ / acetonitrile / 4 h / Heating

With thionyl chloride; sulfuric acid; potassium carbonate; acetic acid; In acetonitrile;
DOI:10.1002/hlca.19970800204