2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane

Base Information

Chemical Name:2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane
CAS No.:308323-79-7
Molecular Formula:C₄₁H₂₆O₂
Molecular Weight:550.656
Hs Code.:

Synonyms:2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane

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Chemical Property of 2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane

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Technology Process of 2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane

There total 1 articles about 2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: phosphoric acid 2-benzenesulfonyl-2-(2-[1,3]dioxolan-2-yl-phenyl)-1-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenyl}-ethyl ester diethyl ester

: 308323-79-7
2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; hexane; at 20 ℃;

Reference yield: 94.0%

: 308323-79-7
2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane

: 308323-68-4
2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-benzaldehyde

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; acetone; at 40 ℃; for 20h;

Reference yield:

: 308323-79-7
2-(2-{2-[2-(2-phenylethynyl-phenylethynyl)-phenylethynyl]-phenylethynyl}-phenyl)-[1,3]dioxolane

: 143215-13-8
α-phenylethynyl-ω-phenylpentakis<1,2-phenylene(2,1-ethynediyl)>

Guidance literature:: Multi-step reaction with 3 steps

1.1: 94 percent / aq. p-TsOH / tetrahydrofuran; acetone / 20 h / 40 °C

2.1: BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

2.2: tetrahydrofuran; hexane / 1 h

3.1: t-BuOK / tetrahydrofuran; hexane / 2 h / 20 °C

With n-butyllithium; potassium tert-butylate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; acetone; 1.1: Hydrolysis / 2.1: Metallation / 2.2: Addition / 3.1: Elimination;