methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate

Base Information

• Chemical Name: methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate
• CAS No.: 900521-34-8
• Molecular Formula: C₃₈H₅₂N₄O₉
• Molecular Weight: 708.852

Synonyms:methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate

Chemical Property of methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate

Chemical Property:

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Technology Process of methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate

There total 2 articles about methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

methyl (2S,5R)-2-(4-allyloxybenzyl)-5-amino-3-aza-9-(tert-butoxycarbonylamino)-4-oxononanoate (900521-33-7) + (2S)-2-acetamido-3-(4-allyloxyphenyl)propanoic acid (171813-89-1) → methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate (900521-34-8)

Guidance literature:

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 16h;

DOI:10.1016/j.tet.2008.09.031

Reference yield: 37.0%

→ methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate (900521-34-8)

Guidance literature:

Reference yield: 55.0%

methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate (900521-34-8) → methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-5-(4-aminobutyl)-3,6,9-triaza-4,7,10-trioxoundecanoate hydrochloride (900521-53-1)

Guidance literature:

methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-3,6,9-triaza-5-(4-[tert-butoxycarbonylamino]butyl)-4,7,10-trioxoundecanoate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;

With hydrogenchloride; In diethyl ether; 1,1,1-trichloroethane; water;

DOI:10.1016/j.tet.2008.09.031

upstream raw materials:

methyl (2S,5R)-2-(4-allyloxybenzyl)-5-amino-3-aza-9-(tert-butoxycarbonylamino)-4-oxononanoate

(2S)-2-acetamido-3-(4-allyloxyphenyl)propanoic acid

Downstream raw materials:

methyl (2S,5R,8S)-2,8-di(4-allyloxybenzyl)-5-(4-aminobutyl)-3,6,9-triaza-4,7,10-trioxoundecanoate hydrochloride

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