p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside

Base Information

• Chemical Name: p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside
• CAS No.: 1042430-58-9
• Molecular Formula: C₂₂H₂₃N₃O₅S
• Molecular Weight: 441.508

Synonyms:p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside

Chemical Property of p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside

Chemical Property:

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Technology Process of p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside

There total 1 articles about p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H23F3O8S2 (1042430-57-8) → p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside (1042430-58-9)

Guidance literature:

With Na₃N; In N,N-dimethyl-formamide; at 80 ℃; for 1h;

DOI:10.1016/j.carres.2007.11.030

Reference yield: 70.0%

p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside (1042430-58-9) + benzyl 2-hydroxyethylcarbamate (77987-49-6) → N-benzyloxycarbonylaminoethyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-β-D-glucopyranoside (1042430-59-0)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 0.75h;

DOI:10.1016/j.carres.2007.11.030

Reference yield:

p-methylphenyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-1-thio-β-D-glucopyranoside (1042430-58-9) → 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-β-D-glucopyranose + 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-α-D-glucopyranose (1314865-08-1)

Guidance literature:

With N-Bromosuccinimide; In acetone; at 0 - 20 ℃; for 2.33333h;

DOI:10.1039/b914534f

upstream raw materials:

C₂₃H₂₃F₃O₈S₂

Downstream raw materials:

N-benzyloxycarbonylaminoethyl 2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-β-D-glucopyranoside

2-O-acetyl-4-azido-3-O-benzoyl-4,6-dideoxy-α-D-glucopyranose

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