2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

Base Information

Chemical Name:2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine
CAS No.:199436-66-3
Molecular Formula:C₂₅H₂₇Cl₂N₅O₇
Molecular Weight:580.425
Hs Code.:

Synonyms:2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

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Chemical Property of 2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

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Technology Process of 2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

There total 6 articles about 2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Oxo-pentanoic acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[6-(2,5-dichloro-phenoxy)-2-isobutyrylamino-purin-9-yl]-tetrahydro-furan-3-yl ester

: 199436-66-3
2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

Guidance literature:: With dichloro-acetic acid; pyrrole; In dichloromethane; for 0.166667h; Yield given;

Reference yield:

: 40608-06-8
levulinic anhydride

: 199436-66-3
2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 16 h / Ambient temperature

2: pyrrole, Cl₂CHCO₂H / CH₂Cl₂ / 0.17 h

With pyridine; dichloro-acetic acid; pyrrole; In dichloromethane;

Reference yield:

: 68892-41-1
5'-O-dimethoxytrityl-N-isobutyryldeoxyguanosine

: 199436-66-3
2'-deoxy-6-O-(2,5-dichlorophenyl)-2-N-isobutyryl-3'-O-levulinylguanosine

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0.5 h / Ambient temperature

2: 1.) mesitylene-2-sulfonyl chloride, 1-methylpyrrolidine, 3.) Et₃N / 1.) 0 deg C, 15 min, 2) 0 deg C, 3 h, 3.) room temperature, H₂O, 16 h

3: pyridine / 16 h / Ambient temperature

4: pyrrole, Cl₂CHCO₂H / CH₂Cl₂ / 0.17 h

With 1-Methylpyrrolidine; pyridine; dichloro-acetic acid; 2-mesitylenesulphonyl chloride; pyrrole; triethylamine; In dichloromethane;