Technology Process of C34H37F5N4O7S
There total 15 articles about C34H37F5N4O7S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 4h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; dimethyl sulfoxide / 2 h / 0 - 50 °C
2.1: trifluoroacetic acid; triethylsilane / 7 h / 0 - 40 °C
3.1: boron tribromide / dichloromethane / 1.16 h / -78 - 20 °C
4.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
4.2: 1 h / 0 - 20 °C / Inert atmosphere
5.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / 90 °C / Inert atmosphere
With
pyridine; triethylsilane; tetrakis(triphenylphosphine) palladium(0); N-benzyl-N,N,N-triethylammonium chloride; boron tribromide; potassium carbonate; trifluoroacetic acid; sodium hydroxide;
In
1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: formic acid; triethylamine / 2 h / 0 - 100 °C
2.1: polyphosphoric acid / 4 h / 80 °C
3.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water; dimethyl sulfoxide / 2 h / 0 - 50 °C
4.1: trifluoroacetic acid; triethylsilane / 7 h / 0 - 40 °C
5.1: boron tribromide / dichloromethane / 1.16 h / -78 - 20 °C
6.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
6.2: 1 h / 0 - 20 °C / Inert atmosphere
7.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 4 h / 90 °C / Inert atmosphere
With
pyridine; triethylsilane; tetrakis(triphenylphosphine) palladium(0); formic acid; N-benzyl-N,N,N-triethylammonium chloride; boron tribromide; potassium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide;