Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl

Base Information

• Chemical Name: Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl
• CAS No.: 207613-97-6
• Molecular Formula: C₃₈H₅₀N₆O₉S
• Molecular Weight: 766.916

Synonyms:Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl

Chemical Property of Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl

Chemical Property:

Purity/Quality:

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Technology Process of Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl

There total 1 articles about Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

BOC-O-benzyl-L-serine (23680-31-1) + H-Arg(Tos)-βAla-OBzl*TFA → Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl (207613-97-6)

Guidance literature:

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1039/a908145c

Reference yield:

Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl (207613-97-6) → H-Ser(Bzl)-Arg(Tos)-βAla-OBzl*HCl

Guidance literature:

With hydrogenchloride; In ethyl acetate;

DOI:10.1039/a908145c

Reference yield:

Boc-Ser(Bzl)-Arg(Tos)-βAla-OBzl (207613-97-6) → Boc-Gly-Ser(Bzl)-Arg(Tos)-βAla-OBzl

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / ethyl acetate

2: 83 percent / NEt₃; BOP / dimethylformamide / 2 h / 20 °C

With hydrogenchloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In ethyl acetate; N,N-dimethyl-formamide; 1: Acidolysis / 2: Acylation;

DOI:10.1039/a908145c

upstream raw materials:

BOC-O-benzyl-L-serine

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