N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester

Base Information

• Chemical Name: N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester
• CAS No.: 122701-29-5
• Molecular Formula: C₅₁H₆₄N₆O₁₂
• Molecular Weight: 953.102

Synonyms:N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester

Chemical Property of N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester

Chemical Property:

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Technology Process of N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester

There total 8 articles about N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N6-[(benzyloxy)carbonyl]-N2-{N 2,N6-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine (614-02-8) + methyl (2S)-2-amino-6-{[(benzyloxy)carbonyl]amino}hexanoate hydrochloride (27894-50-4) → N6-benzyloxycarbonyl-N2-[N6-benzyloxycarbonyl-N2-(N2,N6-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester (122701-29-5)

Guidance literature:

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 14h; Inert atmosphere;

Reference yield:

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine (405-39-0) → N6-benzyloxycarbonyl-N2-[N6-benzyloxycarbonyl-N2-(N2,N6-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester (122701-29-5)

Guidance literature:

Multi-step reaction with 3 steps

2: NaOH; aqueous acetone

3: 1-ethyl-piperidine; THF / anschliessend Behandeln mit N⁶-Benzyloxycarbonyl-L-lysin-methylester, Aethylacetat und wss. KHCO₃

With tetrahydrofuran; 1-ethyl-piperidine; sodium hydroxide; acetone;

DOI:10.1039/jr9530000475

Reference yield:

Nα,Nε-Bis(benzyloxycarbonyl)-L-lysyl-Nε-(benzyloxycarbonyl)-L-lysine Methyl Ester (13523-84-7,97485-07-9) → N6-benzyloxycarbonyl-N2-[N6-benzyloxycarbonyl-N2-(N2,N6-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine methyl ester (122701-29-5)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH; aqueous acetone

2: 1-ethyl-piperidine; THF / anschliessend Behandeln mit N⁶-Benzyloxycarbonyl-L-lysin-methylester, Aethylacetat und wss. KHCO₃

With tetrahydrofuran; 1-ethyl-piperidine; sodium hydroxide; acetone;

DOI:10.1039/jr9530000475

upstream raw materials:

(S)-methyl 2-amino-6-(benzyloxycarbonylamino)hexanoate

N,N'-di-[(phenylmethoxy)carbonyl]-L-lysine

N^α,N^ε-Bis(benzyloxycarbonyl)-L-lysyl-N^ε-(benzyloxycarbonyl)-L-lysine Methyl Ester

N⁶-[(benzyloxy)carbonyl]-N²-{N ²,N⁶-bis[(benzyloxy)carbonyl]-L-lysyl}-L-lysine

Downstream raw materials:

N⁶-benzyloxycarbonyl-N²-[N⁶-benzyloxycarbonyl-N²-(N²,N⁶-bis-benzyloxycarbonyl-L-lysyl)-L-lysyl]-L-lysine

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