cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol

Base Information

Chemical Name:cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol
CAS No.:267665-93-0
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:

Synonyms:cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol

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Technology Process of cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol

There total 10 articles about cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 208114-17-4
(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4-yl)-3-phenyl-prop-2-yn-ol

: 267665-93-0
cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol

Guidance literature:: With hydrogen; P-2 Ni; In ethanol; for 2h; under 760 Torr;
DOI:10.1002/jccs.200000004

Reference yield: 80.0%

: 2-phenyl-3-[(1'R,2'R)-1'-(2',3'-O-isopropylidene-1',2',3'-trihydroxypropyl)]-5,6-dihydro-1,4-dithiin

: 267665-93-0
cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol

Guidance literature:: With Ni-Raney W₂; In acetic acid; for 0.416667h; Ambient temperature;
DOI:10.1016/0040-4020(96)00677-1

Reference yield:

: 4688-38-4
(2R,3S)-1,2-O-isopropylidene-4-pentyne-1,2,3-triol

: 267665-93-0
cis-(1S,5'R)-1-(2',2'-dimethyl-[1',3']dioxolan-4'-yl)-3-phenyl-prop-2-en-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / PdIPh₃P)4; CuI; pyrrolidine / 2.5 h

2: 93 percent / H₂ / P-2 Ni / ethanol / 2 h / 760 Torr

With pyrrolidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; hydrogen; P-2 Ni; In ethanol; 1: Phenylation / 2: Catalytic hydrogenation;
DOI:10.1002/jccs.200000004