Technology Process of 1,3,6,8-tetrakis(4-allylphenyl)pyrene
There total 3 articles about 1,3,6,8-tetrakis(4-allylphenyl)pyrene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,4-dioxane; water;
at 90 ℃;
for 72h;
Inert atmosphere;
DOI:10.1246/cl.2012.316
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 8 h / -30 °C / Inert atmosphere
1.2: -30 - 20 °C / Inert atmosphere
2.1: isopropylmagnesium chloride / tetrahydrofuran / 8 h / 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / 1,4-dioxane; water / 72 h / 90 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); isopropylmagnesium chloride; potassium carbonate;
In
tetrahydrofuran; 1,4-dioxane; water;
3.1: Suzuki coupling;
DOI:10.1246/cl.2012.316
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: isopropylmagnesium chloride / tetrahydrofuran / 8 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / 1,4-dioxane; water / 72 h / 90 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); isopropylmagnesium chloride; potassium carbonate;
In
tetrahydrofuran; 1,4-dioxane; water;
2.1: Suzuki coupling;
DOI:10.1246/cl.2012.316
