C₁₈H₂₉O₄PS

Base Information

• Chemical Name: C₁₈H₂₉O₄PS
• CAS No.: 1356965-48-4
• Molecular Formula: C₁₈H₂₉O₄PS
• Molecular Weight: 372.466
• Mol file: 1356965-48-4.mol

Synonyms:C₁₈H₂₉O₄PS

Chemical Property of C₁₈H₂₉O₄PS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₈H₂₉O₄PS

There total 2 articles about C₁₈H₂₉O₄PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C10H22NO5PS (1356965-39-3) + 4-tert-butylmagnesium bromide (63488-10-8) → C18H29O4PS (1356965-48-4)

Guidance literature:

In tetrahydrofuran; at -78 - 0 ℃; Inert atmosphere;

DOI:10.1021/ja210758n

Reference yield:

C9H19O5PS (1356965-38-2) → C18H29O4PS (1356965-48-4)

Guidance literature:

Multi-step reaction with 2 steps

1: isopropyl magnesium chloride - lithium chloride complex / tetrahydrofuran / 0.33 h / -20 °C / Inert atmosphere

2: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

With isopropyl magnesium chloride - lithium chloride complex; In tetrahydrofuran;

DOI:10.1021/ja210758n

Reference yield: 92.0%

C18H29O4PS (1356965-48-4) → C18H31O4PS (1356965-64-4)

Guidance literature:

With borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1021/ja210758n

upstream raw materials:

C₉H₁₉O₅PS

C₁₀H₂₂NO₅PS

4-tert-butylmagnesium bromide

Downstream raw materials:

C₁₈H₃₁O₄PS

C₁₄H₂₀O₂S