methylphenylisopropoxyborane

Base Information

Chemical Name:methylphenylisopropoxyborane
CAS No.:97782-78-0
Molecular Formula:C₁₀H₁₅BO₂
Molecular Weight:178.039
Hs Code.:

Synonyms:methylphenylisopropoxyborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methylphenylisopropoxyborane

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Technology Process of methylphenylisopropoxyborane

There total 2 articles about methylphenylisopropoxyborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4406-77-3
2-Phenyl-1,3,2-dioxaborinane

: 917-54-4
methyllithium

: 97782-78-0
methylphenylisopropoxyborane

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: LiCl; 2 equiv of MeLi slowly adding to a soln. of the boronic ester at -78°C, stirring for 3 h at the same temp., 1 equiv of anhydrous HCl in Et2O adding, warming to room temp., stirring for 15 min; the content was detd. by (11)B NMR spectrum;
DOI:10.1021/om00129a019

Reference yield: 92.0%

: 591-51-5
phenyllithium

: 51901-48-5
2-methyl-[1,3,2]dioxaborinane

: 97782-78-0
methylphenylisopropoxyborane

: 59073-99-3
methyldiphenylborane

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: LiCl; 1 equiv of PhLi slowly adding to a soln. of the boronic ester at -78°C, stirring for 3 h at the same temp., 1 equiv of anhydrous HCl in Et2O adding, warming to room temp., stirring for 15 min; the content was detd. by (11)B NMR spectrum;
DOI:10.1021/om00129a019