C₁₂H₁₅NO₃

Base Information

Chemical Name:C₁₂H₁₅NO₃
CAS No.:1187028-00-7
Molecular Formula:C₁₂H₁₅NO₃
Molecular Weight:221.256
Hs Code.:

C<sub>12</sub>H<sub>15</sub>NO<sub>3</sub>

Synonyms:C₁₂H₁₅NO₃

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Chemical Property of C₁₂H₁₅NO₃

Chemical Property:

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Technology Process of C₁₂H₁₅NO₃

There total 5 articles about C₁₂H₁₅NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1187027-99-1
C₁₄H₁₇NO₄

: 1187028-00-7
C₁₂H₁₅NO₃

Guidance literature:: C₁₄H₁₇NO₄; With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 0.166667h; Inert atmosphere;

With water; rochelle salt; In tetrahydrofuran; ethyl acetate; toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol901349b

Reference yield:

: C₁₀H₁₁NO₃

: 1187028-00-7
C₁₂H₁₅NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: propionic acid / 140 °C

2: diisobutylaluminium hydride / tetrahydrofuran / -78 °C

With diisobutylaluminium hydride; propionic acid; In tetrahydrofuran;
DOI:10.1021/ja5102739

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 1187028-00-7
C₁₂H₁₅NO₃

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / water; ethanol; diethyl ether

2: toluene-4-sulfonic acid / toluene; water / Reflux

3: lithium perchlorate; sodium tetrahydroborate / ethanol

4: propionic acid / 140 °C

5: diisobutylaluminium hydride / tetrahydrofuran / -78 °C

With sodium tetrahydroborate; lithium perchlorate; diisobutylaluminium hydride; toluene-4-sulfonic acid; propionic acid; sodium hydroxide; In tetrahydrofuran; diethyl ether; ethanol; water; toluene;
DOI:10.1021/ja5102739