di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate

Base Information

Chemical Name:di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate
CAS No.:101040-09-9
Molecular Formula:C₂₉H₄₈NO₁₀P
Molecular Weight:601.675
Hs Code.:

di(tert-butyl) <(1S)-2-benzyloxy-1-<N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-N-hydroxyamino>ethyl>phosphonate

Synonyms:di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate

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Technology Process of di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate

There total 3 articles about di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 13086-84-5
di-tert-butyl phosphite

: 101062-05-9
2-benzyloxy-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)ethanimine

: di(tert-butyl) <(1R)-2-benzyloxy-1-ethyl>phosphonate

: 101040-09-9
di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate

Guidance literature:: With lithium tert-butoxide; In dichloromethane; at -60 - -20 ℃; for 2h; Yield given;
DOI:10.1002/hlca.19850680629

Reference yield:

: 35023-80-4
2,3:5,6-di-O-isopropylidene-D-mannose oxime

: 101040-09-9
di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 86.5 percent / CHCl₃ / 15 h

2: 68 percent / t-BuOLi / CH₂Cl₂ / 2 h / -60 - -20 °C

With lithium tert-butoxide; In dichloromethane; chloroform;
DOI:10.1002/hlca.19850680629

Reference yield:

: 60656-87-3
benzyloxyacetoaldehyde

: 101040-09-9
di(tert-butyl) <(1S)-2-benzyloxy-1-ethyl>phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 86.5 percent / CHCl₃ / 15 h

2: 68 percent / t-BuOLi / CH₂Cl₂ / 2 h / -60 - -20 °C

With lithium tert-butoxide; In dichloromethane; chloroform;
DOI:10.1002/hlca.19850680629