7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester

Base Information

Chemical Name:7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester
CAS No.:444188-89-0
Molecular Formula:C₁₇H₂₅N₂O₅P
Molecular Weight:368.37
Hs Code.:

Synonyms:7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester

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Chemical Property of 7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester

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Technology Process of 7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester

There total 9 articles about 7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

: 66207-08-7,1624258-63-4
3,4-epoxy-piperidine-1-carboxylic acid benzyl ester

: 814-49-3
diethyl chlorophosphate

: 98-59-9
p-toluenesulfonyl chloride

: 444188-89-0
7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester

Guidance literature:: 3,4-epoxy-piperidine-1-carboxylic acid benzyl ester; With sodium azide; water; ammonium chloride; In methanol; at 65 ℃; for 18h;

p-toluenesulfonyl chloride; With pyridine; In methanol; dichloromethane; at 0 - 20 ℃; for 68h;

diethyl chlorophosphate; Further stages;

Reference yield: 21.0%

: 444188-88-9
benzyl 3,7-diazabicyclo[4.1.0]heptane-3-carboxylate

: 814-49-3
diethyl chlorophosphate

: 444188-89-0
7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 24h;

Reference yield:

: 66207-08-7,1624258-63-4
3,4-epoxy-piperidine-1-carboxylic acid benzyl ester

: 814-49-3
diethyl chlorophosphate

: 444188-89-0
7-(diethoxyphosphoryl)-3,7-diazabicyclo[4.1.0]heptane-3-carboxylic acid benzyl ester

Guidance literature:: 3,4-epoxy-piperidine-1-carboxylic acid benzyl ester; With sodium azide; ammonium chloride; In methanol; water; for 20h; Heating;

With pyridine; p-toluenesulfonyl chloride; In dichloromethane; at 0 - 20 ℃;

diethyl chlorophosphate;