Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

Base Information

Chemical Name:Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide
CAS No.:438044-95-2
Molecular Formula:C₂₃H₃₆N₄O₅
Molecular Weight:448.563
Hs Code.:

Synonyms:Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

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Chemical Property of Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

Chemical Property:

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Technology Process of Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

There total 1 articles about Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129739-09-9
4-methyl-2S-[(morpholine-4-carbonyl)amino]pentanoic acid

: 294885-32-8
2S-amino-N-methoxy-N-methyl-4-phenyl-butyramide

: 438044-95-2
Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

Guidance literature:: 4-methyl-2S-[(morpholine-4-carbonyl)amino]pentanoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -30 - -15 ℃; for 0.25h;

2S-amino-N-methoxy-N-methyl-4-phenyl-butyramide; In tetrahydrofuran; for 0.5h;
DOI:10.1016/S0968-0896(02)00468-6

Reference yield: 91.0%

: 438044-95-2
Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

: 438044-70-3
1-((1-formyl-3-phenylpropylcarbamoyl)-3-methylbutyl)morpholine-4-carboxamide

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at -30 - -20 ℃; for 0.5h;
DOI:10.1016/S0968-0896(02)00468-6

Reference yield:

: 438044-95-2
Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(methoxy-methyl-carbamoyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

: 900813-43-6
Morpholine-4-carboxylic acid {(S)-1-[(S)-1-(benzoyl-hydrazonomethyl)-3-phenyl-propylcarbamoyl]-3-methyl-butyl}-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / LiAlH₄ / diethyl ether; tetrahydrofuran / 0.5 h / -30 - -20 °C

2: 32 percent / ethanol / 4 h / Heating

With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; ethanol;
DOI:10.1016/S0968-0896(02)00468-6