N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

Base Information

Chemical Name:N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide
CAS No.:1013212-26-4
Molecular Formula:C₁₉H₂₇NO₄S
Molecular Weight:365.494
Hs Code.:

Synonyms:N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

Suppliers and Price of N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

There total 1 articles about N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1013212-25-3
C₁₂H₂₁NO₂

: 98-59-9
p-toluenesulfonyl chloride

: 1013212-26-4
N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/j.tetlet.2007.12.097

Reference yield: 90.0%

: 1013212-26-4
N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

: 106-95-6
allyl bromide

: 1013212-27-5
C₂₂H₃₁NO₄S

Guidance literature:: With sodium hydride; In tetrahydrofuran; dimethyl sulfoxide; at 0 - 20 ℃; for 16h;
DOI:10.1016/j.tetlet.2007.12.097

Reference yield: 89.0%

: 1013212-26-4
N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide

: 106-96-7
propargyl bromide

: 1224301-21-6
N₁-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methylbenzenesulfonamide

Guidance literature:: N-{(1R)-1-[(2S)-1,4-dioxaspiro[4.5]dec-2-yl]-3-butenyl}-4-methyl-1-benzenesulfonamide; With sodium hydride; In tetrahydrofuran; dimethyl sulfoxide; at 0 - 20 ℃; Inert atmosphere;

propargyl bromide; In tetrahydrofuran; dimethyl sulfoxide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.02.001