[1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester

Base Information

Chemical Name:[1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester
CAS No.:922722-55-2
Molecular Formula:C₁₉H₂₈N₄O₂
Molecular Weight:344.457
Hs Code.:

Synonyms:[1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester

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Chemical Property of [1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester

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Technology Process of [1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester

There total 8 articles about [1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(1-azido-2-phenyl-ethyl)-3-methyl-butylamine

: 50715-28-1
cyclopentyl chloroformate

: 922722-55-2
[1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester

Guidance literature:: With triethanolamine; In water; toluene; at 20 ℃; for 1h;
DOI:10.1021/jm060754+

Reference yield:

: 6921-34-2
benzylmagnesium chloride

: 922722-55-2
[1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: CuBr*DMS / tetrahydrofuran / 0.17 h / -78 °C

1.2: tetrahydrofuran / 3.17 h / -78 - 20 °C

2.1: 92 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3.1: 64 percent / NaN₃ / dimethylformamide / 16 h / 60 °C

4.1: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

5.1: triethanolamine / toluene; H₂O / 1 h / 20 °C

With sodium azide; copper(I) bromide dimethylsulfide complex; triethanolamine; triethylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm060754+

Reference yield:

: 922722-23-4
(3-methyl-1-phenylacetyl-butyl)-carbamic acid tert-butyl ester

: 922722-55-2
[1-(1-azido-2-phenyl-ethyl)-3-methyl-butyl]-carbamic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / NaBH₄ / methanol / -22 - 20 °C

2: 92 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3: 64 percent / NaN₃ / dimethylformamide / 16 h / 60 °C

4: trifluoroacetic acid / CH₂Cl₂ / 0.5 h / 0 °C

5: triethanolamine / toluene; H₂O / 1 h / 20 °C

With sodium tetrahydroborate; sodium azide; triethanolamine; triethylamine; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm060754+