phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside

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Chemical Name:phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside
CAS No.:1319717-02-6
Molecular Formula:C₁₉H₁₈N₆O₃S
Molecular Weight:410.456
Hs Code.:

Synonyms:phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside

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Chemical Property of phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside

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Technology Process of phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside

There total 4 articles about phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 1319717-03-7
phenyl 2,3-diazido-2,3-dideoxy-1-thio-β-D-mannopyranoside

: 1319717-02-6
phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 20 ℃;
DOI:10.1021/jo201179p

Reference yield:

: 1319717-00-4
phenyl 4,6-di-O-acetyl-2,3-diazido-2,3-dideoxy-1-thio-β-D-mannopyranoside

: 1319717-02-6
phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 1.5 h

1.2: Amberlite-H⁺

2.1: toluene-4-sulfonic acid / acetonitrile / 20 °C

With sodium methylate; toluene-4-sulfonic acid; In methanol; acetonitrile;
DOI:10.1021/jo201179p

Reference yield:

: 108-98-5
thiophenol

: 1319717-02-6
phenyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-1-thio-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / 1,2-dichloro-ethane / 5 h / 50 °C

2.1: sodium methylate / methanol / 1.5 h

2.2: Amberlite-H⁺

3.1: toluene-4-sulfonic acid / acetonitrile / 20 °C

With boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; In methanol; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1021/jo201179p