N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline

Base Information

• Chemical Name: N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline
• CAS No.: 223115-52-4
• Molecular Formula: C₃₂H₃₃N₃O
• Molecular Weight: 475.634

Synonyms:N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline

Chemical Property of N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline

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Technology Process of N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline

There total 6 articles about N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

1,3,3-Trimethyl-2-methyleneindoline (118-12-7) + 4-(4-(diethylamino)phenyl)-2-(hydroxyimino)naphthalen-1(2H)-one (223116-23-2) → N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline (223115-52-4)

Guidance literature:

In ethanol; at 100 ℃; for 3h; sealed tube;

DOI:10.1080/00397910903457423

Reference yield: 49.0%

1,3,3-Trimethyl-2-methyleneindoline (118-12-7) + 4--1,2-naphthoquinone (123135-53-5) → N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline (223115-52-4)

Guidance literature:

4--1,2-naphthoquinone; With hydroxylamine hydrochloride; In ethanol; at 20 ℃; for 1h;

1,3,3-Trimethyl-2-methyleneindoline; With sodium acetate; at 80 ℃; for 5h;

DOI:10.1080/00397910903457423

Reference yield:

1,3,3-Trimethyl-2-methyleneindoline (118-12-7) + C20H20N2O2*ClH → N,N-diethyl-4-(1,3,3-trimethylspiro[indoline-2,2'-naphtho[1,2-b][1,4]oxazine]-6'-yl)aniline (223115-52-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; at 120 ℃; for 0.333333h;

DOI:10.1071/CH12435

upstream raw materials:

1,3,3-Trimethyl-2-methyleneindoline

4-(4-(diethylamino)phenyl)-2-(hydroxyimino)naphthalen-1(2H)-one

4--1,2-naphthoquinone

1,2-naphthoquinone

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