9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine

Base Information

Chemical Name:9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine
CAS No.:1200462-34-5
Molecular Formula:C₂₂H₂₄ClN₅O₈
Molecular Weight:521.914
Hs Code.:

Synonyms:9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine

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Chemical Property of 9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine

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Technology Process of 9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine

There total 19 articles about 9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 1200461-10-4
(R/S)-1-(2,6-dinitrophenyl)-2-methyl-1-propanol

: 1201544-68-4
9-[β-D-3‘,5‘-O-bis-(tert-butyldimethylsilyl)-2’-deoxyribofuranosyl]-6-chloro-7-chloromethyl-7-deazapurine

: 1200462-34-5
9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine

: 9-[β-D-3'-O-(tert-butyldimethylsilyl)-2'-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methyl-propyloxy]methyl-7-deazapurine

Guidance literature:: In dichloromethane; at 108 ℃; for 0.5h; Heating;

Reference yield:

: 6-chloro-7-[1-(2,6-dinitrophenyl)-2-methyl-propyloxy]methyl-7-deazapurine-2'-deoxyribonucleoside

: 1200462-34-5
9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield:

: 1200461-10-4
(R/S)-1-(2,6-dinitrophenyl)-2-methyl-1-propanol

: 1201544-68-4
9-[β-D-3‘,5‘-O-bis-(tert-butyldimethylsilyl)-2’-deoxyribofuranosyl]-6-chloro-7-chloromethyl-7-deazapurine

: 1200462-34-5
9-[β-D-2′-deoxyribofuranosyl]-6-chloro-7-[1-(2,6-dinitrophenyl)-2-methylpropyloxy]methyl-7-deazapurine

Guidance literature:: (R/S)-1-(2,6-dinitrophenyl)-2-methyl-1-propanol; 9-[β-D-3‘,5‘-O-bis-(tert-butyldimethylsilyl)-2’-deoxyribofuranosyl]-6-chloro-7-chloromethyl-7-deazapurine; at 108 ℃; for 0.5h; Neat (no solvent); Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 2h;
DOI:10.1002/anie.201106516