1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde

Base Information

Chemical Name:1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde
CAS No.:123475-02-5
Molecular Formula:C₁₉H₂₆O₅
Molecular Weight:334.412
Hs Code.:

Synonyms:1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde

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Chemical Property of 1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde

Chemical Property:

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Technology Process of 1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde

There total 6 articles about 1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 123475-00-3
{1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentyl}-methanol

: 123475-02-5
1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde

Guidance literature:: With pyridine-SO₃ complex; triethylamine; In dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)80627-4

Reference yield:

: 4460-86-0,14374-62-0
asaraldehyde

: 123475-02-5
1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / LDA / tetrahydrofuran

2: 97 percent / NaBH₄-CeCl₃*7H₂O / methanol

3: 88 percent / NaH / dimethylformamide

4: 93 percent / DIBAL-H / tetrahydrofuran

5: 96 percent / SO₃*Py, Et₃N / dimethylsulfoxide

With sodium tetrahydroborate; cerium(III) chloride; pyridine-SO₃ complex; sodium hydride; diisobutylaluminium hydride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)80627-4

Reference yield:

: 28247-15-6
ethyl 1-acetylcyclopropane-1-carboxylate

: 123475-02-5
1-[(E)-1-Methoxy-3-(2,4,5-trimethoxy-phenyl)-allyl]-cyclopentanecarbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / LDA / tetrahydrofuran

2: 97 percent / NaBH₄-CeCl₃*7H₂O / methanol

3: 88 percent / NaH / dimethylformamide

4: 93 percent / DIBAL-H / tetrahydrofuran

5: 96 percent / SO₃*Py, Et₃N / dimethylsulfoxide

With sodium tetrahydroborate; cerium(III) chloride; pyridine-SO₃ complex; sodium hydride; diisobutylaluminium hydride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)80627-4