C₆₆H₅₈O₂₀

Base Information

• Chemical Name: C₆₆H₅₈O₂₀
• CAS No.: 1046825-12-0
• Molecular Formula: C₆₆H₅₈O₂₀
• Molecular Weight: 1171.17
• Mol file: 1046825-12-0.mol

Synonyms:C₆₆H₅₈O₂₀

Chemical Property of C₆₆H₅₈O₂₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₆H₅₈O₂₀

There total 1 articles about C₆₆H₅₈O₂₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

benzyl-5-O-acetyl-α-D-arabinofuranoside (1046825-04-0) + 2,3-5-tri-O-benzoyl-α-D-arabinofuranosyl 2,2,2-trichloroacetimidate → C66H58O20 (1046825-12-0)

Guidance literature:

benzyl-5-O-acetyl-α-D-arabinofuranoside; 2,3-5-tri-O-benzoyl-α-D-arabinofuranosyl 2,2,2-trichloroacetimidate; In dichloromethane; for 0.25h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 - 20 ℃; Inert atmosphere;

DOI:10.1039/b803409e

Reference yield: 94.0%

C66H58O20 (1046825-12-0) → 5-O-acetyl-[2,3,5-tri-O-benzoyl-α-D-(1->2)-arabinofuranosyl]-[2,3,5-tri-O-benzoyl-α-D-(1->3)-arabinofuranosyl]-D-arabinofuranose (1046825-05-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 18h; under 750.075 Torr;

DOI:10.1039/b803409e

upstream raw materials:

benzyl-5-O-acetyl-α-D-arabinofuranoside

Downstream raw materials:

5-O-acetyl-[2,3,5-tri-O-benzoyl-α-D-(1->2)-arabinofuranosyl]-[2,3,5-tri-O-benzoyl-α-D-(1->3)-arabinofuranosyl]-D-arabinofuranose