C₈H₁₅ClMgSi

Base Information

Chemical Name:C₈H₁₅ClMgSi
CAS No.:145029-02-3
Molecular Formula:C₈H₁₅ClMgSi
Molecular Weight:199.051
Hs Code.:

Synonyms:C₈H₁₅ClMgSi

Suppliers and Price of C₈H₁₅ClMgSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₈H₁₅ClMgSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₈H₁₅ClMgSi

There total 1 articles about C₈H₁₅ClMgSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5272-33-3
2-methyl-4-(trimethylsilyl)but-3-yn-2-ol

: 145029-02-3
C₈H₁₅ClMgSi

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 1 h / 20 °C

2: magnesium / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With hydrogenchloride; magnesium; In tetrahydrofuran; water;
DOI:10.1021/jacs.0c09323

Reference yield:

: 145029-02-3
C₈H₁₅ClMgSi

: 5389-87-7
1-chloro-3,7-dimethylocta-2,6-diene

: 90544-18-6
(5E,9E)-1-trimethylsilyl-3,3,6,10-tetramethylundeca-5,9-dien-1-yne

: 90544-11-9
[(E)-4,8-Dimethyl-1-(2-methyl-propenylidene)-nona-3,7-dienyl]-trimethyl-silane

Guidance literature:: In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 0 ℃;
DOI:10.1016/S0040-4039(01)80019-8

Reference yield:

: 145029-02-3
C₈H₁₅ClMgSi

: 1-(3-fluoro-3-methylbut-1-en-2-yl)-4-nitrobenzene

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride / diethyl ether / 3 h / 0 °C / Inert atmosphere

3: potassium carbonate / methanol / 2 h / 20 °C

4: phosphorus tribromide; tetraethylammonium bromide; water / dichloromethane / 4 h / Reflux

5: potassium carbonate; palladium diacetate; XPhos / water; acetonitrile / 18 h / 80 °C / Inert atmosphere

6: 4-tolyl iodide; pyridinium polyhydrogenfluoride; 3-chloro-benzenecarboperoxoic acid / chloroform / 24 h / -10 °C

With lithium aluminium tetrahydride; pyridinium polyhydrogenfluoride; 4-tolyl iodide; tetraethylammonium bromide; water; palladium diacetate; phosphorus tribromide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; XPhos; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; water; acetonitrile; 5: |Suzuki Coupling;
DOI:10.1021/jacs.0c09323