C₃₃H₃₉F₅O₈

Base Information

Chemical Name:C₃₃H₃₉F₅O₈
CAS No.:891845-44-6
Molecular Formula:C₃₃H₃₉F₅O₈
Molecular Weight:658.66
Hs Code.:

C<sub>33</sub>H<sub>39</sub>F<sub>5</sub>O<sub>8</sub>

Synonyms:C₃₃H₃₉F₅O₈

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Chemical Property of C₃₃H₃₉F₅O₈

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Technology Process of C₃₃H₃₉F₅O₈

There total 5 articles about C₃₃H₃₉F₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₄₄O₆Si

: 891845-44-6
C₃₃H₃₉F₅O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: nBuLi / hexane; tetrahydrofuran / 1 h / 0 °C

1.2: hexane; tetrahydrofuran / 18 h / -78 - 25 °C

2.1: 60 percent / Grubbs' catalyst II / CH₂Cl₂ / 14 h / 40 °C

3.1: tetra-n-butylammonium fluoride / tetrahydrofuran / 14 h / 25 °C

4.1: (COCl)2; dimethyl sulfoxide; Et₃N / CH₂Cl₂ / -78 - 0 °C

5.1: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 1 h / 25 °C

6.1: dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h / 25 °C

With sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; oxalyl dichloride; tetrabutyl ammonium fluoride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; hexane; dichloromethane; water; tert-butyl alcohol; 4.1: Swern oxidation;
DOI:10.1002/anie.200600295

Reference yield:

: C₂₇H₄₀O₈

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 891845-44-6
C₃₃H₃₉F₅O₈

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1002/anie.200600295

Reference yield:

: 947392-70-3
C₂₇H₄₂O₇

: 891845-44-6
C₃₃H₃₉F₅O₈

Guidance literature:: Multi-step reaction with 3 steps

1: (COCl)2; dimethyl sulfoxide; Et₃N / CH₂Cl₂ / -78 - 0 °C

2: NaClO₂; NaH₂PO₄; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 1 h / 25 °C

3: dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h / 25 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; In dichloromethane; water; tert-butyl alcohol; 1: Swern oxidation;
DOI:10.1002/anie.200600295