1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone

Base Information

• Chemical Name: 1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone
• CAS No.: 129375-13-9
• Molecular Formula: C₁₆H₂₄O₂
• Molecular Weight: 248.365

Synonyms:1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone

Chemical Property of 1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone

Chemical Property:

Purity/Quality:

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Technology Process of 1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone

There total 2 articles about 1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

2-(1,1-dimethylethyl)-5-methyl-4-(1-methylethyl)phenyl ethanoate (129375-08-2) → 1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone (129375-13-9)

Guidance literature:

With titanium tetrachloride; In chlorobenzene; at 100 ℃; for 2h;

DOI:10.1007/BF00809536

Reference yield:

6-tert-butyl-4-isopropyl-3-methylphenol (30061-94-0) → 1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone (129375-13-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent

2: 23 percent / TiCl₄ / chlorobenzene / 2 h / 100 °C

With titanium tetrachloride; In chlorobenzene;

DOI:10.1007/BF00809536

Reference yield: 84.0%

1-<3-(1,1-dimethylethyl)-2-hydroxy-6-methyl-5-(1-methylethyl)phenyl>-ethanone (129375-13-9) → 1-<6-hydroxy-2-methyl-3-(1-methylethyl)phenyl>-ethanone (105337-35-7)

Guidance literature:

With aluminium trichloride; In nitromethane; at 20 ℃; for 24h;

DOI:10.1007/BF00809536

upstream raw materials:

2-(1,1-dimethylethyl)-5-methyl-4-(1-methylethyl)phenyl ethanoate

6-tert-butyl-4-isopropyl-3-methylphenol

Downstream raw materials:

1-<6-hydroxy-2-methyl-3-(1-methylethyl)phenyl>-ethanone

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