N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

Base Information

Chemical Name:N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine
CAS No.:932740-15-3
Molecular Formula:C₂₈H₃₉N₇O₆
Molecular Weight:569.661
Hs Code.:

N<sup>6</sup>-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

Synonyms:N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

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Chemical Property of N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

Chemical Property:

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Technology Process of N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

There total 6 articles about N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 932740-12-0
N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-2',3'-isopropylidene-5'-oxo-5'-deoxyadenosine

: 932740-15-3
N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 70 ℃; for 0.75h;
DOI:10.1021/jm061279i

Reference yield:

: 2140-11-6
2',3'-O-isopropylideneinosine

: 932740-15-3
N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / 2,2,6,6-tetramethyl-1-piperidinyloxy free radical; iodosobenzene diacetate / acetonitrile; H₂O / 4 h / 20 °C

2: SOCl₂; DMF / CHCl₃ / 5 h / Heating

3: 941 mg / tetrahydrofuran / 0.5 h / 5 - 20 °C

4: 81 percent / diisopropylethylamine / ethanol / 18 h / Heating

5: 67 percent / aq. HCl / dioxane / 0.75 h / 70 °C

With hydrogenchloride; thionyl chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; ethanol; chloroform; water; acetonitrile;
DOI:10.1021/jm061279i

Reference yield:

: 103201-21-4
6-chloro-6-deoxy-5'-ethylamino-2',3'-isopropylidene-5'-oxo-5'-deoxyinosine

: 932740-15-3
N⁶-(8-benzyloxycarbonylaminooctyl)-5'-ethylamino-5'-oxo-5'-deoxyadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / diisopropylethylamine / ethanol / 18 h / Heating

2: 67 percent / aq. HCl / dioxane / 0.75 h / 70 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; ethanol;
DOI:10.1021/jm061279i