[((C₃H₃N₂)3BH)Ru(NHC(C₆H₅)2)(CH₂P(C₃H₇)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(C₃₆H₅₃BN₇P₂)][B(C₆H₅)4]

Base Information

• Chemical Name: [((C₃H₃N₂)3BH)Ru(NHC(C₆H₅)2)(CH₂P(C₃H₇)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(C₃₆H₅₃BN₇P₂)][B(C₆H₅)4]
• CAS No.: 286431-03-6
• Molecular Formula: C₂₄H₂₀B*C₃₆H₅₃BN₇P₂Ru
• Molecular Weight: 1076.93

Synonyms:[((C₃H₃N₂)3BH)Ru(NHC(C₆H₅)2)(CH₂P(C₃H₇)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(C₃₆H₅₃BN₇P₂)][B(C₆H₅)4]

Chemical Property of [((C₃H₃N₂)3BH)Ru(NHC(C₆H₅)2)(CH₂P(C₃H₇)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(C₃₆H₅₃BN₇P₂)][B(C₆H₅)4]

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Technology Process of [((C₃H₃N₂)3BH)Ru(NHC(C₆H₅)2)(CH₂P(C₃H₇)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(C₃₆H₅₃BN₇P₂)][B(C₆H₅)4]

There total 1 articles about [((C₃H₃N₂)3BH)Ru(NHC(C₆H₅)2)(CH₂P(C₃H₇)2)2]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Ru(C₃₆H₅₃BN₇P₂)][B(C₆H₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Benzophenone imine (1013-88-3) + [(hydrotris(pyrazolyl)borate)RuCl(1,2-bis(diisopropylphosphino)ethane)] (192201-49-3) + sodium tetraphenyl borate (143-66-8) → [((C3H3N2)3BH)Ru(NHC(C6H5)2)(CH2P(C3H7)2)2](1+)*B(C6H5)4(1-)=[Ru(C36H53BN7P2)][B(C6H5)4] (286431-03-6)

Guidance literature:

In methanol; mixt. with excess NaBPh4 stirred with gentle heating for 30 min, color changed to deep yellow, stirred at room temp. for 2 h, concd., cooled o -20°C; ppt. filtered off, washed with ethanol and ether, dried in vac., elem. anal.;

DOI:10.1016/S0020-1693(00)00002-5

Reference yield: 66.0%

[((C3H3N2)3BH)Ru(NHC(C6H5)2)(CH2P(C3H7)2)2](1+)*B(C6H5)4(1-)=[Ru(C36H53BN7P2)][B(C6H5)4] (286431-03-6) → [(hydrotris(pyrazolyl)borate)Ru(σ-η1-C6H4C(C6H5)=NH)(1,2-bis(diisopropylphosphino)ethane)2] (286431-09-2)

Guidance literature:

With K(OC(CH₃)3); In tetrahydrofuran; ruthenium complex treated with excess reagent, stirred at room temp. for 15 min, solvent removed; residue extd. with petroleum ether, filtered (Celite), concd., cooled to -20°C, ppt. filtered off, dried in vac., elem. anal.;

DOI:10.1016/S0020-1693(00)00002-5

upstream raw materials:

Benzophenone imine

[(hydrotris(pyrazolyl)borate)RuCl(1,2-bis(diisopropylphosphino)ethane)]

sodium tetraphenyl borate

Downstream raw materials:

[(hydrotris(pyrazolyl)borate)Ru(σ-η1-C6H4C(C6H5)=NH)(1,2-bis(diisopropylphosphino)ethane)2]

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