8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside
CAS No.:79726-91-3
Molecular Formula:C₃₉H₅₀O₉
Molecular Weight:662.821
Hs Code.:

Synonyms:8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

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Technology Process of 8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 1 articles about 8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 65827-59-0
2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl chloride

: 34957-73-8
methyl 9-hydroxynonanoate

: 79726-91-3
8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: With 2,4,6-trimethyl-pyridine; silver trifluoromethanesulfonate; In nitromethane; toluene; at -20 ℃; for 15h;
DOI:10.1016/S0008-6215(00)84694-7

Reference yield: 97.0%

: 79726-91-3
8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

: 109681-57-4
8-(Methoxycarbonyl)octyl 3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: With sodium methylate; In methanol; for 4h;

Reference yield:

: 79726-91-3
8-methoxycarbonyloct-1-yl 2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranoside

: 79726-93-5
9-[(2R,4aR,6S,7S,8S,8aR)-7-Acetoxy-8-((2R,3R,5R,6R)-3,5-bis-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy]-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) H2; 2.) α,α-dimethoxytoluene, p-toluenesulfonic acid / 1.) palladium-on-charcoal (10percent) / 1.) ethanol (95percent), 400 kPa; 2.) acetonitrile, 30 min

2: tetraethylammonium bromide / dimethylformamide; CH₂Cl₂ / Ambient temperature

With benzaldehyde dimethyl acetal; tetraethylammonium bromide; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)84694-7