2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal

Base Information

Chemical Name:2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal
CAS No.:222191-90-4
Molecular Formula:C₄₀H₄₂O₄S₂
Molecular Weight:650.903
Hs Code.:

Synonyms:2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal

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Chemical Property of 2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal

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Technology Process of 2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal

There total 3 articles about 2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

: 197716-38-4
2,3,5-tri-O-benzyl-1-O-methyl-D-xylofuranoside

: 100-53-8
phenylmethanethiol

: 1-S-benzyl 2,3,5-tri-O-benzyl-D-xylo-furanoside

: 222191-90-4
2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal

Guidance literature:: In hydrogenchloride; for 72h; Ambient temperature;
DOI:10.1002/(SICI)1099-0690(199903)1999:3<691::AID-EJOC691>3.0.CO;2-J

Reference yield:

: 1824-96-0,1824-97-1,3795-68-4,3795-69-5,4229-54-3,5531-18-0,7473-45-2,13039-63-9,13039-64-0,13039-65-1,13039-67-3,22416-73-5,22861-09-2,25129-51-5,52485-92-4,52689-55-1,52689-56-2,56607-40-0,72880-70-7,79083-42-4,86782-30-1,86782-31-2,89615-03-2,89673-67-6,89707-99-3,102045-32-9,135910-17-7
methyl xylofuranoside

: 222191-90-4
2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide

2: 84 percent / aq. HCl / 72 h / Ambient temperature

With sodium hydride; In hydrogenchloride; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1099-0690(199903)1999:3<691::AID-EJOC691>3.0.CO;2-J

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-xylofuranose

: 222191-90-4
2,3,5-tri-O-benzyl-D-xylose dibenzyl dithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: H⁺

2: NaH / dimethylformamide

3: 84 percent / aq. HCl / 72 h / Ambient temperature

With hydrogen cation; sodium hydride; In hydrogenchloride; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1099-0690(199903)1999:3<691::AID-EJOC691>3.0.CO;2-J