[2.2]paracyclophane-4,15-N,N'-diphenyldiamine

Base Information

Chemical Name:[2.2]paracyclophane-4,15-N,N'-diphenyldiamine
CAS No.:1412449-13-8
Molecular Formula:C₂₈H₂₆N₂
Molecular Weight:390.528
Hs Code.:

Synonyms:[2.2]paracyclophane-4,15-N,N'-diphenyldiamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2.2]paracyclophane-4,15-N,N'-diphenyldiamine

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Technology Process of [2.2]paracyclophane-4,15-N,N'-diphenyldiamine

There total 2 articles about [2.2]paracyclophane-4,15-N,N'-diphenyldiamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 196316-30-0,196316-31-1,23927-40-4,96392-77-7
4,16-dibromo[2.2]paracyclophane

: 62-53-3
aniline

: 1412449-13-8
[2.2]paracyclophane-4,15-N,N'-diphenyldiamine

Guidance literature:: With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; In toluene; at 110 ℃; for 20h; Glovebox;
DOI:10.1039/c2dt31497e

Reference yield: 50.0%

: 196316-30-0,196316-31-1,23927-40-4,96392-77-7
4,16-dibromo[2.2]paracyclophane

: 62-53-3
aniline

: 1633-22-3
[2.2]Paracyclophan

: 1412449-13-8
[2.2]paracyclophane-4,15-N,N'-diphenyldiamine

Guidance literature:: With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; 4-(4-dicyclohexanylphosphinyl[2.2]paracyclophan-13-yl)morpholine borane complex; sodium t-butanolate; In toluene; at 110 ℃; for 12h; Reagent/catalyst; Inert atmosphere;
DOI:10.1039/c7ob02393f