3,4-bis-2-<(allylthio)methyl>furan

Base Information

• Chemical Name: 3,4-bis-2-<(allylthio)methyl>furan
• CAS No.: 96194-68-2
• Molecular Formula: C₂₄H₂₆O₃S
• Molecular Weight: 394.535

Synonyms:3,4-bis-2-<(allylthio)methyl>furan

Chemical Property of 3,4-bis-2-<(allylthio)methyl>furan

Chemical Property:

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Technology Process of 3,4-bis-2-<(allylthio)methyl>furan

There total 1 articles about 3,4-bis-2-<(allylthio)methyl>furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3,4-Bis-benzyloxymethyl-furan-2-yl)-methanethiol + allyl bromide (106-95-6) → 3,4-bis-2-<(allylthio)methyl>furan (96194-68-2)

Guidance literature:

With sodium hydride; Multistep reaction; 1.) THF, RT, 30 min;

DOI:10.1021/jo00210a046

Reference yield: 84.0%

3,4-bis-2-<(allylthio)methyl>furan (96194-68-2) → (1R,5R,7S)-8,9-Bis-benzyloxymethyl-10-oxa-3-thia-tricyclo[5.2.1.01,5]dec-8-ene (96194-76-2)

Guidance literature:

In toluene; at 110 ℃; for 24h;

DOI:10.1021/jo00210a046

upstream raw materials:

allyl bromide

Downstream raw materials:

(1R,5R,7S)-8,9-Bis-benzyloxymethyl-10-oxa-3-thia-tricyclo[5.2.1.0^1,5]dec-8-ene

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