1-{2-[(E)-2-(t-butoxycarbonyl)ethenyl]-6-[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole

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Chemical Name:1-{2-[(E)-2-(t-butoxycarbonyl)ethenyl]-6-[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole
CAS No.:1187529-49-2
Molecular Formula:C₂₅H₂₆N₂O₂
Molecular Weight:386.494
Hs Code.:

Synonyms:1-{2-[(E)-2-(t-butoxycarbonyl)ethenyl]-6-[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole

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Chemical Property of 1-{2-[(E)-2-(t-butoxycarbonyl)ethenyl]-6-[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole

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Technology Process of 1-{2-[(E)-2-(t-butoxycarbonyl)ethenyl]-6-[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole

There total 1 articles about 1-{2-[(E)-2-(t-butoxycarbonyl)ethenyl]-6-[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 622-97-9,24936-41-2
1-ethenyl-4-methylbenzene

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1126-00-7
1-phenylpyrazole

: 1187529-49-2
1-{2-[(E)-2-(t-butoxycarbonyl)ethenyl]-6-[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole

: 1187529-39-0
1-{2,6-bis[(E)-2-(4-methylphenyl)ethenyl]phenyl}-1H-pyrazole

Guidance literature:: 1-ethenyl-4-methylbenzene; 1-phenylpyrazole; With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;

tert-Butyl acrylate; In N,N-dimethyl-formamide; at 100 ℃; for 2h;

With bis(benzonitrile)palladium(II) dichloride; In 1,3,5-trimethyl-benzene; at 150 ℃; for 15h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo901485v