(1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate

Base Information

• Chemical Name: (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate
• CAS No.: 244607-57-6
• Molecular Formula: C₃₀H₄₈O₂Si
• Molecular Weight: 468.795

Synonyms:(1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate

Chemical Property of (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate

Chemical Property:

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Technology Process of (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate

There total 1 articles about (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

n-octyne (629-05-0) + Trimethylsilanyl-propynoic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester → (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate (244607-57-6)

Guidance literature:

Trimethylsilanyl-propynoic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester; With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; at -78 - -50 ℃;

n-octyne; In diethyl ether; at -50 ℃;

With hydrogenchloride; In diethyl ether;

DOI:10.1021/ja9905694

Reference yield: 90.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate (244607-57-6) → 8-hexyl-1,3-dioxo-2-phenyl-5-trimethylsilanyl-2,3,5,8-tetrahydro-1H-[1,2,4]triazolo[1,2-a]pyridazine-6-carboxylic acid 5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:

In dichloromethane; at -30 ℃;

DOI:10.1021/ja9905694

Reference yield: 69.0%

nonan-1-al (124-19-6) + (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate (244607-57-6) → (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (2R,3R)-2-[(trimethylsilyl)methyl]-2-[(E)-1-octenyl]-3-hydroxyundecanoate + (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (2S,3R)-2-[(trimethylsilyl)methyl]-2-[(E)-1-octenyl]-3-hydroxyundecanoate + (1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (2S,3S)-2-[(trimethylsilyl)methyl]-2-[(E)-1-octenyl]-3-hydroxyundecanoate

Guidance literature:

(1R,2S,5R)-2-(1-methyl-1-phenethyl)-5-methylcyclohexyl (3E)-2-[(Z)-(trimethylsilyl)methylene]-3-decenoate; With titanium(IV) isopropylate; isopropylmagnesium chloride; In diethyl ether; at -20 ℃; for 20h;

nonan-1-al; In diethyl ether; at -20 ℃; for 2h;

DOI:10.1021/ja0341844

upstream raw materials:

n-octyne

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