1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate

Base Information

Chemical Name:1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate
CAS No.:1374964-70-1
Molecular Formula:C₂₄H₂₄BrNO₄
Molecular Weight:470.363
Hs Code.:

Synonyms:1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate

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Chemical Property of 1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate

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Technology Process of 1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate

There total 1 articles about 1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1374964-66-5
1-tert-butyl 2-ethyl 3-benzoyl-5-bromo-1H-indole-1,2-dicarboxylate

: 27200-84-6
methyl triphenylphosphonium bromide

: 1374964-74-5
ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-2-carboxylate

: 1374964-70-1
1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate

Guidance literature:: methyl triphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere;

1-tert-butyl 2-ethyl 3-benzoyl-5-bromo-1H-indole-1,2-dicarboxylate; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ml3000462

Reference yield: 41.0%

: 75-11-6
diiodomethane

: 1374964-70-1
1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate

: 1374964-80-3
ethyl 5-bromo-3-(1-phenylcyclopropyl)-1H-indole-2-carboxylate

Guidance literature:: diiodomethane; With diethylzinc; trifluoroacetic acid; In dichloromethane; for 0.333333h; Inert atmosphere;

1-tert-butyl 2-ethyl 5-bromo-3-(1-phenylvinyl)-1H-indole-1,2-dicarboxylate; In dichloromethane; for 2h; Inert atmosphere;
DOI:10.1021/ml3000462