benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside
CAS No.:74615-24-0
Molecular Formula:C₅₆H₅₉NO₁₁
Molecular Weight:922.085
Hs Code.:

Synonyms:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside

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Chemical Property of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside

There total 1 articles about benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 74615-21-7
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-glucopyranosyl)-α-D-glucopyranoside

: 74615-22-8
N-[(2S,3R,4R,5S,6R)-2,4-Bis-benzyloxy-6-benzyloxymethyl-5-((2S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3,3-dihydroxy-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

: 74615-24-0
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside

Guidance literature:: With dimethyl sulfoxide; In acetic acid; Ambient temperature;
DOI:10.1016/S0008-6215(00)85521-4

Reference yield:

: 74615-24-0
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside

: 74615-23-9
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-mannopyranosyl)-α-D-glucopyranoside

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; for 4h; Yield given; Ambient temperature;
DOI:10.1016/S0008-6215(00)85521-4

Reference yield:

: 74615-24-0
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4,6-tri-O-benzyl-β-D-arabino-hexopyranosyl-2-ulose)-α-D-glucopyranoside

: 186765-90-2
2-acetamido-2-deoxy-4-O-(β-D-mannopyranosyl)-β-D-glucosamine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium borohydride / CH₂Cl₂; methanol / 4 h / Ambient temperature

2: 90 percent / H₂ / palladium-on-charcoal (10percent) / acetic acid / 48 h / 1520 Torr / Ambient temperature

With sodium tetrahydroborate; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetic acid;
DOI:10.1016/S0008-6215(00)85521-4