N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Base Information

Chemical Name:N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol
CAS No.:205649-43-0
Molecular Formula:C₃₇H₄₀N₂O₄S
Molecular Weight:608.802
Hs Code.:

Synonyms:N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

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Technology Process of N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

There total 3 articles about N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69567-11-9,76738-52-8,126836-30-4
2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 205649-43-0
N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: Multi-step reaction with 4 steps

1: DCC / CH₂Cl₂ / 16 h / 24 °C

2: 412 mg / BH₃*THF / ethyl acetate / 16 h / 24 °C

3: 412 mg / TFA / CH₂Cl₂ / 0.5 h / 24 °C

4: 1.) Et₃N, 2.) Et₃N, 2-chloro-1-methylpyridinium iodide / 1.) CH₂Cl₂, 24 deg C, 1 h, 2.) CH₂Cl₂, 24 deg C, 2.5 h

With borane-THF; 2-chloro-1-methyl-pyridinium iodide; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(98)00966-1

Reference yield:

: 205649-38-3
N--2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 205649-43-0
N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: Multi-step reaction with 2 steps

1: 412 mg / TFA / CH₂Cl₂ / 0.5 h / 24 °C

2: 1.) Et₃N, 2.) Et₃N, 2-chloro-1-methylpyridinium iodide / 1.) CH₂Cl₂, 24 deg C, 1 h, 2.) CH₂Cl₂, 24 deg C, 2.5 h

With 2-chloro-1-methyl-pyridinium iodide; triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/S0040-4020(98)00966-1

Reference yield:

: 205649-36-1
N--2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

: 205649-43-0
N-(2-isothiocyanatoethyl)-2,3,4,6-tetra-O-benzyl-1,5-dideoxy-1,5-imino-D-glucitol

Guidance literature:: Multi-step reaction with 3 steps

1: 412 mg / BH₃*THF / ethyl acetate / 16 h / 24 °C

2: 412 mg / TFA / CH₂Cl₂ / 0.5 h / 24 °C

3: 1.) Et₃N, 2.) Et₃N, 2-chloro-1-methylpyridinium iodide / 1.) CH₂Cl₂, 24 deg C, 1 h, 2.) CH₂Cl₂, 24 deg C, 2.5 h

With borane-THF; 2-chloro-1-methyl-pyridinium iodide; triethylamine; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4020(98)00966-1