(S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide

Base Information

Chemical Name:(S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide
CAS No.:471283-18-8
Molecular Formula:C₁₆H₂₆N₄O₂
Molecular Weight:306.408
Hs Code.:

Synonyms:(S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide

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Technology Process of (S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide

There total 5 articles about (S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 471283-16-6
{1-[2-(2-tert-butoxycarbonylamino-3-methyl-butyrylamino)-phenylcarbamoyl]-2-methyl-propyl}-carbamic acid tert-butyl ester

: 471283-18-8
(S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/S0040-4039(02)00687-1

Reference yield: 66.0%

: C₃₂H₃₈N₄O₆

: 471283-18-8
(S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 ℃; for 8h;
DOI:10.1021/acs.inorgchem.6b01066

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 471283-18-8
(S)-2-Amino-N-[2-((S)-2-amino-3-methyl-butyrylamino)-phenyl]-3-methyl-butyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / dicyclohexyl carbodiimide / ethyl acetate / 6 h / 20 °C

2: 98 percent / CF₃COOH / CH₂Cl₂ / 0.5 h / 20 °C

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate;
DOI:10.1016/S0040-4039(02)00687-1