2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid

Base Information

• Chemical Name: 2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid
• CAS No.: 1228293-88-6
• Molecular Formula: C₂₃H₂₆O₅
• Molecular Weight: 382.456

Synonyms:2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid

Chemical Property of 2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid

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Technology Process of 2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid

There total 1 articles about 2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C24H28O5 (1228293-99-9) → 2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid (1228293-88-6)

Guidance literature:

C₂₄H₂₈O₅; With potassium trimethylsilonate; In diethyl ether; at 20 ℃; for 2.16667h;

With hydrogenchloride; In diethyl ether; water; pH=4;

DOI:10.1002/anie.201000624

Reference yield: 94.0%

(4S,6S)-6-methoxy-8-methylnon-8-en-4-ol (1228293-89-7) + 2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid (1228293-88-6) → C34H46O6 (1228293-86-4)

Guidance literature:

2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

(4S,6S)-6-methoxy-8-methylnon-8-en-4-ol; With dmap; In toluene; at 20 ℃; for 0.5h;

DOI:10.1002/anie.201000624

Reference yield: 77.0%

2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid (1228293-88-6) + (S)-Non-8-en-4-ol (143617-63-4) → (S)-non-8-en-4-yl 2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetate

Guidance literature:

2-((2R,4R,6S)-4-((benzyloxy)methoxy)-6-((E)-styryl)tetrahydro-2H-pyran-2-yl)acetic acid; With 2,4,6-trichlorobenzoyl chloride; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Cooling with ice;

(S)-Non-8-en-4-ol; With dmap; In toluene; at 20 ℃;

upstream raw materials:

C₂₄H₂₈O₅

Downstream raw materials:

C₃₄H₄₆O₆

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