C₁₃H₁₇NO

Base Information

Chemical Name:C₁₃H₁₇NO
CAS No.:1608506-34-8
Molecular Formula:C₁₃H₁₇NO
Molecular Weight:203.284
Hs Code.:

Synonyms:C₁₃H₁₇NO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₇NO

Chemical Property:

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Technology Process of C₁₃H₁₇NO

There total 3 articles about C₁₃H₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 127983-04-4
C₁₅H₁₉NO₂

: 1608506-34-8
C₁₃H₁₇NO

Guidance literature:: With potassium borohydride; lithium chloride; In tetrahydrofuran; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/ol501058a

Reference yield:

: 127983-02-2
(2-cyano-ethyl)-phenethyl-malonic acid diethyl ester

: 1608506-34-8
C₁₃H₁₇NO

Guidance literature:: Multi-step reaction with 2 steps

1: lithium chloride / dimethyl sulfoxide / 4 h / 140 °C / Inert atmosphere

2: lithium chloride; potassium borohydride / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

With potassium borohydride; lithium chloride; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/ol501058a

Reference yield:

: 6628-68-8
ethyl 2-(ethoxycarbonyl)-4-phenylbutanoate

: 1608506-34-8
C₁₃H₁₇NO

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / mineral oil; dimethyl sulfoxide; tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

1.2: 60 h / Inert atmosphere

2.1: lithium chloride / dimethyl sulfoxide / 4 h / 140 °C / Inert atmosphere

3.1: lithium chloride; potassium borohydride / tetrahydrofuran / 24 h / Inert atmosphere; Reflux

With potassium borohydride; sodium hydride; lithium chloride; In tetrahydrofuran; dimethyl sulfoxide; mineral oil;
DOI:10.1021/ol501058a