3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine

Base Information

Chemical Name:3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine
CAS No.:887127-65-3
Molecular Formula:C₅₈H₇₂I₂N₄O₄S₂
Molecular Weight:1207.18
Hs Code.:

Synonyms:3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine

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Chemical Property of 3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine

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Technology Process of 3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine

There total 7 articles about 3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 887127-64-2
3,6-didodecyl-2,7-diiodophenantrene-9,10-quinone

: 23680-12-8
N,N′-(4,5-diamino-1,2-phenylene)bis(4-methylbenzenesulfonamide)

: 887127-65-3
3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine

Guidance literature:: With acetic acid; In ethanol; Reflux;
DOI:10.1016/j.tetlet.2011.11.121

Reference yield:

: 887127-61-9
3,6-dibromophenantrene-9,10-di(ethyleneglycol)ketal

: 887127-65-3
3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: t-BuLi / tetrahydrofuran; diethyl ether; pentane / 0.33 h / -78 - -30 °C

1.2: 6.58 g / tetrahydrofuran; diethyl ether; pentane / -78 - 20 °C

2.1: H₂O; TsOH / CH₂Cl₂; acetonitrile / Heating

3.1: 5.34 g / NIS; TFA / 3 h / Heating

4.1: acetic acid / ethanol / 2 h / Heating

With N-iodo-succinimide; water; tert.-butyl lithium; toluene-4-sulfonic acid; acetic acid; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; acetonitrile; pentane;
DOI:10.1021/ja058514r

Reference yield:

: 887127-63-1
3,6-didodecylphenantrene-9,10-quinone

: 887127-65-3
3,6-didodecyl-2,7-diiodo-11,12-bis(p-toluenesulfonamido)dibenzo[a,c]phenazine

Guidance literature:: Multi-step reaction with 2 steps

1: 5.34 g / NIS; TFA / 3 h / Heating

2: acetic acid / ethanol / 2 h / Heating

With N-iodo-succinimide; acetic acid; trifluoroacetic acid; In ethanol;
DOI:10.1021/ja058514r