C₆₅H₈₈O₁₂

Base Information

Chemical Name:C₆₅H₈₈O₁₂
CAS No.:115352-20-0
Molecular Formula:C₆₅H₈₈O₁₂
Molecular Weight:1061.41
Hs Code.:

C<sub>65</sub>H<sub>88</sub>O<sub>12</sub>

Synonyms:C₆₅H₈₈O₁₂

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Chemical Property of C₆₅H₈₈O₁₂

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Technology Process of C₆₅H₈₈O₁₂

There total 18 articles about C₆₅H₈₈O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 104307-11-1
C₆₈H₉₂O₁₂

: 115352-20-0
C₆₅H₈₈O₁₂

Guidance literature:: With acetic acid; In tetrahydrofuran; at 50 ℃; for 36h;
DOI:10.1016/S0040-4020(01)86918-0

Reference yield:

: 104307-04-2
C₅₁H₇₀O₁₀Si

: 115352-20-0
C₆₅H₈₈O₁₂

Guidance literature:: Multi-step reaction with 13 steps

1: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

2: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

3: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

4: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

5: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

6: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

7: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

8: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

9: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂, -78 to 0 deg C

10: 1) sec-BuLi / 1) THF, hexane, -78 deg C, 10 min, 2) THF,hexane, -78 deg C, 20 min.

11: pyridine / 55 °C

12: 5percent sodium amalgam / ethyl acetate; methanol

13: 63 percent / AcOH,H₂O / tetrahydrofuran / 36 h / 50 °C

With pyridine; sodium tetrahydroborate; sodium amalgam; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; pyridinium p-toluenesulfonate; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0

Reference yield:

: 104307-03-1
C₅₇H₇₆O₁₂SSi

: 115352-20-0
C₆₅H₈₈O₁₂

Guidance literature:: Multi-step reaction with 15 steps

1: CrO₃*2pyridine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: aluminum amalgam / tetrahydrofuran / Ambient temperature

3: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

4: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

5: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

6: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

7: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

8: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

9: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

10: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

11: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, -78 deg C, 15 min, 2) CH₂Cl₂, -78 to 0 deg C

12: 1) sec-BuLi / 1) THF, hexane, -78 deg C, 10 min, 2) THF,hexane, -78 deg C, 20 min.

13: pyridine / 55 °C

14: 5percent sodium amalgam / ethyl acetate; methanol

15: 63 percent / AcOH,H₂O / tetrahydrofuran / 36 h / 50 °C

With pyridine; sodium tetrahydroborate; sodium amalgam; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; aluminium amalgam; tetrabutyl ammonium fluoride; hydrogen; sec.-butyllithium; pyridinium p-toluenesulfonate; dipyridine chromium trioxide; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0