12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole

Base Information

Chemical Name:12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole
CAS No.:1357150-57-2
Molecular Formula:C₄₅H₃₄N₂
Molecular Weight:602.778
Hs Code.:

Synonyms:12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole

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Chemical Property of 12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole

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Technology Process of 12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole

There total 4 articles about 12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.4%

: 1257220-44-2
7-bromo-12,12-dimethyl-10-phenyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1357150-57-2
12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 73 ℃; for 5h; Inert atmosphere;

Reference yield:

: 1257220-43-1
12,12-dimethyl-10-phenyl-10,12-dihydroindeno[2,1-b]carbazole

: 1357150-57-2
12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 5 h / 73 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1257220-47-5
12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 1357150-57-2
12,12-dimethyl-10-phenyl-7-(4-diphenylaminophenyl)-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogensulfite; copper; 3,5-ditertbutyl salicylic acid; potassium carbonate / 10 h / 170 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide

3: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water; ethanol / 5 h / 73 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 3,5-ditertbutyl salicylic acid; copper; potassium carbonate; sodium hydrogensulfite; In ethanol; water; N,N-dimethyl-formamide; toluene;