N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester

Base Information

Chemical Name:N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester
CAS No.:135321-13-0
Molecular Formula:C₂₂H₂₆N₂O₅
Molecular Weight:398.459
Hs Code.:

Synonyms:N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester

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Chemical Property of N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester

Chemical Property:

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Technology Process of N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester

There total 2 articles about N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27019-47-2
β-alanine benzyl ester p-toluenesulfonate

: 111331-82-9
3-[(tert-butoxycarbonyl)amino]benzoic acid

: 135321-13-0
N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester

Guidance literature:: With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; Multistep reaction; 1.) CH₂Cl₂, 0 deg C, 3 h, 2.) CH₂Cl₂, RT, 12 h;
DOI:10.1021/jm00101a017

Reference yield:

: 135321-13-0
N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester

: N-(m-aminobenzoyl)-β-alanine benzyl ester trifluoroacetate

Guidance literature:

Reference yield:

: 135321-13-0
N-[m-(1-t-butoxyformamido)benzoyl]-β-alanine benzyl ester

: 3-{3-[2-Amino-3-(4-carbamimidoyl-phenyl)-propionylamino]-benzoylamino}-propionic acid

Guidance literature:: Multi-step reaction with 6 steps

1: trifluoroacetic acid (TFA) / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.)2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine (NMM), 2.) N-methylmorpholine (NMM) / 1.) CH₂Cl₂, 0 deg C, 3 h, 2.) CH₂Cl₂, RT, 12 h

3: H₂S, triethylamine (TEA) / pyridine / Ambient temperature

4: acetone / 50 °C

5: ammonium acetate / methanol / 70 °C

6: H₂ / 5percent Pd/C / acetic acid / 760 Torr

With 4-methyl-morpholine; ammonium acetate; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; hydrogen sulfide; hydrogen; triethylamine; trifluoroacetic acid; palladium on activated charcoal; In pyridine; methanol; dichloromethane; acetic acid; acetone;
DOI:10.1021/jm00101a017