methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate

Base Information

Chemical Name:methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate
CAS No.:221077-44-7
Molecular Formula:C₂₄H₃₆N₂O₈
Molecular Weight:480.558
Hs Code.:

Synonyms:methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate

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Chemical Property of methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate

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Technology Process of methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate

There total 1 articles about methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 96-32-2
bromoacetic acid methyl ester

: 221077-43-6
methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-hydroxybenzoate

: 221077-44-7
methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate

Guidance literature:: With potassium carbonate; In acetone; at 50 ℃; for 16h;
DOI:10.1021/jm010393s

Reference yield: 68.0%

: 221077-44-7
methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate

: 103-49-1
dibenzylamine

: 2-(carboxymethoxy)-5-[(2S)-2-{[(dibenzylamino)carbonyl]amino}-3-oxo-3-(pentylamino)propyl]benzoic acid

Guidance literature:: methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1h;

With triethylamine; trichloromethyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.25h;

dibenzylamine; With lithium hydroxide; more than 3 stages;

Reference yield: 67.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 221077-44-7
methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate

: 221077-46-9
5-[(S)-2-((S)-2-tert-Butoxycarbonylamino-3-phenyl-propionylamino)-2-pentylcarbamoyl-ethyl]-2-methoxycarbonylmethoxy-benzoic acid methyl ester

Guidance literature:: methyl 5-[(2S)-2-[(tert-butoxycarbonyl)amino]-3-oxo-3-(pentylamino)propyl]-2-(2-methoxy-2-oxoethoxy)benzoate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

N-tert-butoxycarbonyl-L-phenylalanine; With triethylamine; In dichloromethane;

With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 0 - 20 ℃;