N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine

Base Information

• Chemical Name: N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine
• CAS No.: 1219835-49-0
• Molecular Formula: C₃₃H₃₇N₃O₈
• Molecular Weight: 603.672

Synonyms:N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine

Chemical Property of N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine

Chemical Property:

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Technology Process of N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine

There total 1 articles about N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine benzyl ester (1219835-29-6) → N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine (1219835-49-0)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; water; for 20h;

DOI:10.1016/j.bmc.2010.01.009

Reference yield: 93.0%

N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine (1219835-49-0) → N-((3S)-N-(L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine (1219834-98-6)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 0 - 20 ℃; under 750.075 Torr; Inert atmosphere;

DOI:10.1016/j.bmc.2010.01.009

upstream raw materials:

N-((3S)-N-(Boc-L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine benzyl ester

Downstream raw materials:

N-((3S)-N-(L-tyrosinyl)-1,2,3,4-tetrahydroisoquinoline-3-carbonyl)-L-tyrosine

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