7-(8-chloro-3-(3-Methylenecyclobutyl)iMidazo[1,5-a]pyrazin-1-yl)-2-phenylquinoline

Base Information

• Chemical Name: 7-(8-chloro-3-(3-Methylenecyclobutyl)iMidazo[1,5-a]pyrazin-1-yl)-2-phenylquinoline
• CAS No.: 867163-50-6
• Molecular Formula: C₂₆H₁₉ClN₄
• Molecular Weight: 422.917
• Mol file: 867163-50-6.mol

Synonyms:7-[8-chloro-3-(3-methylenecyclobutyl)imidazo[1,5-a]pyrazin-1-yl]-2-phenylquinoline

Chemical Property of 7-(8-chloro-3-(3-Methylenecyclobutyl)iMidazo[1,5-a]pyrazin-1-yl)-2-phenylquinoline

Chemical Property:

Purity/Quality:

≥95% ^*data from raw suppliers

7-(8-Chloro-3-(3-methylenecyclobutyl)imidazo[1,5-a]pyrazin-1-yl)-2-phenylquinoline 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 7-(8-chloro-3-(3-Methylenecyclobutyl)iMidazo[1,5-a]pyrazin-1-yl)-2-phenylquinoline

There total 1 articles about 7-(8-chloro-3-(3-Methylenecyclobutyl)iMidazo[1,5-a]pyrazin-1-yl)-2-phenylquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-[(3-chloropyrazin-2-yl)(2-phenylquinolin-7-yl)methyl]-3-methylenecyclobutanecarboxamide (867163-52-8) → 7-[8-chloro-3-(3-methylenecyclobutyl)imidazo[1,5-a]pyrazin-1-yl]-2-phenylquinoline (867163-50-6)

Guidance literature:

With trichlorophosphate; In N,N-dimethyl-formamide; acetonitrile; at 55 ℃; for 2h;

DOI:10.1016/j.bmc.2007.10.061

Reference yield: 62.0%

7-[8-chloro-3-(3-methylenecyclobutyl)imidazo[1,5-a]pyrazin-1-yl]-2-phenylquinoline (867163-50-6) → {3-[8-chloro-1-(2-phenylquinolin-7-yl)imidazo[1,5-a]pyrazin-3-yl]cyclobutyl}methanol (867163-48-2)

Guidance literature:

7-[8-chloro-3-(3-methylenecyclobutyl)imidazo[1,5-a]pyrazin-1-yl]-2-phenylquinoline; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 - 20 ℃;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 0 - 20 ℃; Further stages.;

DOI:10.1016/j.bmc.2007.10.061

Reference yield:

7-[8-chloro-3-(3-methylenecyclobutyl)imidazo[1,5-a]pyrazin-1-yl]-2-phenylquinoline (867163-50-6) → 3-[8-chloro-1-(2-phenylquinolin-7-yl)-imidazo[1,5-a]pyrazin-3-yl]-1-hydroxymethyl-cyclobutanol (867163-54-0)

Guidance literature:

With potassium osmate(VI); 4-methylmorpholine N-oxide; In tetrahydrofuran; water; at 20 ℃; for 20h;

upstream raw materials:

N-[(3-chloropyrazin-2-yl)(2-phenylquinolin-7-yl)methyl]-3-methylenecyclobutanecarboxamide

Downstream raw materials:

3-[8-chloro-1-(2-phenyl-quinolin-7-yl)-imidazo[1,5-a]pyrazin-3-yl]-1-methyl-cyclobutanol

3-[8-chloro-1-(2-phenylquinolin-7-yl)-imidazo[1,5-a]pyrazin-3-yl]-1-hydroxymethyl-cyclobutanol

{3-[8-amino-1-(2-phenylquinolin-7-yl)imidazo[1,5-a]pyrazin-3-yl]cyclobutyl}methanol

{3-[8-chloro-1-(2-phenylquinolin-7-yl)imidazo[1,5-a]pyrazin-3-yl]cyclobutyl}methanol

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