C₁₂H₁₀N₂O₄

Base Information

Chemical Name:C₁₂H₁₀N₂O₄
CAS No.:1393556-49-4
Molecular Formula:C₁₂H₁₀N₂O₄
Molecular Weight:246.222
Hs Code.:

C<sub>12</sub>H<sub>10</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₂H₁₀N₂O₄

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Chemical Property of C₁₂H₁₀N₂O₄

Chemical Property:

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Technology Process of C₁₂H₁₀N₂O₄

There total 3 articles about C₁₂H₁₀N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₁₈N₂O₈

: 1393556-49-4
C₁₂H₁₀N₂O₄

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 5h;
DOI:10.1016/j.bmcl.2012.10.050

Reference yield:

: 2150-37-0
methyl 3,5-dimethoxybenzoate

: 1393556-49-4
C₁₂H₁₀N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C

2.1: triethylamine; diphenyl phosphoryl azide / 80 °C

3.1: sodium hydroxide; benzoic acid / tetrahydrofuran / 0.5 h / 20 °C

4.1: sodium nitrite; hydrogenchloride / tetrahydrofuran; water / 0 - 5 °C

4.2: 1 h / 0 - 5 °C

5.1: boron tribromide / dichloromethane

5.2: 3 h / 20 °C

6.1: sodium methylate; methanol / 5 h / 20 °C

With hydrogenchloride; methanol; diphenyl phosphoryl azide; sodium methylate; boron tribromide; triethylamine; benzoic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 2.1: |Curtius Rearrangement / 3.1: |Curtius Rearrangement;
DOI:10.1016/j.bmcl.2012.10.050

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1393556-49-4
C₁₂H₁₀N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / acetonitrile / 20 °C

2.1: sodium hydroxide / 1,4-dioxane / 5 h / 20 °C

3.1: triethylamine; diphenyl phosphoryl azide / 80 °C

4.1: sodium hydroxide; benzoic acid / tetrahydrofuran / 0.5 h / 20 °C

5.1: sodium nitrite; hydrogenchloride / tetrahydrofuran; water / 0 - 5 °C

5.2: 1 h / 0 - 5 °C

6.1: boron tribromide / dichloromethane

6.2: 3 h / 20 °C

7.1: sodium methylate; methanol / 5 h / 20 °C

With hydrogenchloride; methanol; diphenyl phosphoryl azide; sodium methylate; boron tribromide; potassium carbonate; triethylamine; benzoic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile; 3.1: |Curtius Rearrangement / 4.1: |Curtius Rearrangement;
DOI:10.1016/j.bmcl.2012.10.050