9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

Base Information

Chemical Name:9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate
CAS No.:1260095-56-4
Molecular Formula:C₅₅H₆₆N₄O₁₁
Molecular Weight:959.149
Hs Code.:

9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

Synonyms:9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

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Chemical Property of 9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

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Technology Process of 9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

There total 1 articles about 9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1260095-54-2
1,3-bis(methoxymethyl)aniline

: 798576-99-5
4-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-4-(2-carboxyethyl)heptanedioic acid

: 1260095-56-4
9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

Guidance literature:: 4-(((9H-fluoren-9-yl)methoxy)carbonylamino)-4-(2-carboxyethyl)heptanedioic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

1,3-bis(methoxymethyl)aniline; In N,N-dimethyl-formamide; at 20 ℃; for 28h;
DOI:10.1021/ja106076h

Reference yield: 90.0%

: 1260095-56-4
9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

: 1260095-60-0
4-amino-N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)heptanediamide

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/ja106076h

Reference yield:

: 1260095-56-4
9H-fluoren-9-ylmethyl 1,7-bis(3,5-bis(methoxymethyl)phenylamino)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)-1,7-dioxoheptan-4-ylcarbamate

: 1260095-64-4
4-(2,2-diphenylbenzo[d][1,3]dioxole-5-carboxamido)-N₁,N₇-bis(3,5-bis(methoxymethyl)phenyl)-4-(3-(3,5-bis(methoxymethyl)phenylamino)-3-oxopropyl)heptanediamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: piperidine / N,N-dimethyl-formamide / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 0 °C

2.2: 48 h / 20 °C

With piperidine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1021/ja106076h