4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one

Base Information

Chemical Name:4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one
CAS No.:1361960-07-7
Molecular Formula:C₂₂H₂₃BrO
Molecular Weight:383.328
Hs Code.:

Synonyms:4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one

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Chemical Property of 4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one

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Technology Process of 4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one

There total 5 articles about 4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 195259-08-6
4-mesitylbutan-2-one

: 85020-75-3
1-(4-bromophenyl)-2-propyn-1-ol

: 1361960-07-7
4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one

: 1361960-50-0
C₂₂H₂₃BrO

Guidance literature:: With silver hexafluoroantimonate; dichloro(pyridine-2-carboxylato)gold(III); In 1,2-dichloro-ethane; at 50 ℃; for 1h; regioselective reaction; Molecular sieve;
DOI:10.1021/jo300147u

Reference yield:

: 1122594-14-2
1-(4-bromophenyl)-3-(trimethylsilyl)prop-2-yn-1-ol

: 1361960-07-7
4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one

: 1361960-50-0
C₂₂H₂₃BrO

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; potassium carbonate / 2 h / 20 °C

2: dichloro(pyridine-2-carboxylato)gold(III); silver hexafluoroantimonate / 1,2-dichloro-ethane / 1 h / 50 °C / Molecular sieve

With methanol; silver hexafluoroantimonate; dichloro(pyridine-2-carboxylato)gold(III); potassium carbonate; In 1,2-dichloro-ethane;
DOI:10.1021/jo300147u

Reference yield:

: 1225870-58-5
C₁₆H₂₂O₃

: 1361960-07-7
4-(3-(3-(4-bromophenyl)propa-1,2-dienyl)-2,4,6-trimethylphenyl)butan-2-one

: 1361960-50-0
C₂₂H₂₃BrO

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 2.5 h / 70 °C

2: dichloro(pyridine-2-carboxylato)gold(III); silver hexafluoroantimonate / 1,2-dichloro-ethane / 1 h / 50 °C / Molecular sieve

With silver hexafluoroantimonate; dichloro(pyridine-2-carboxylato)gold(III); sodium hydroxide; In water; 1,2-dichloro-ethane;
DOI:10.1021/jo300147u